ThuliumV1, Main, Exploration, bibRecord, 000A39

Synthesis and Characterization of Three New Zipper‐like Lanthanide [Ln = TmIII, NdIII, CeIII] Coordination Polymers Containing 1,3‐Benzenedicarboxylate and 2‐Phenyl‐1H‐1,3,7,8‐tetraazacyclopenta[l]phenanthrene Ligands

Identifieur interne : 000A39 ( Main/Exploration ); précédent : 000A38; suivant : 000A40

Synthesis and Characterization of Three New Zipper‐like Lanthanide [Ln = TmIII, NdIII, CeIII] Coordination Polymers Containing 1,3‐Benzenedicarboxylate and 2‐Phenyl‐1H‐1,3,7,8‐tetraazacyclopenta[l]phenanthrene Ligands

Auteurs : Xiang-Cheng Wang [République populaire de Chine] ; Chun-Bo Liu [République populaire de Chine] ; Jing Chen [République populaire de Chine] ; Xiu-Ying Li [République populaire de Chine] ; Guang-Bo Che [République populaire de Chine] ; Yong-Sheng Yan [République populaire de Chine]

Source :

ZAAC ‐ Journal of Inorganic and General Chemistry [ 0044-2313 ] ; 2011-05.

RBID : ISTEX:64F536190EE72E2B223AD8ED80B997757D7EE9BB

Descripteurs français

Wicri :
- topic : Collecte de données, Polymère.

English descriptors

Abstract

Reaction of the ligands 2‐phenyl‐1H‐1,3,7,8‐tetraazacyclopenta[l]phenanthrene (PTCP) and benzene‐1,3‐dicarboxylic acid (m‐H2BDC) with Ln2O3 under hydrothermal conditions lead to three isomorphous coordination polymers [Ln2(PTCP)2(m‐BDC)3·H2O]n (Ln = Tm, 1; Nd, 2; Ce, 3). The coordination polymers crystallize in monoclinic, space group P21/m with a = 9.8340(2), b = 17.9140(4), c = 15.6050(3) Å, β = 100.51(3)° for 1, with a = 9.8423(3), b = 18.3562(4), c = 15.6209(3) Å, β = 102.138(3)° for 2, and with a = 9.8620(2), b = 18.4960(4), c = 15.6530(3) Å, β = 102.42(3)° for 3, respectively. The metal ions (Ln3+) are located in an octacoordinated environment and the dinuclear [Ln2O12N4] units act as octahedral secondary building units (SBU), which are bridged in two coordination modes by six m‐BDC ligands to form a three‐strand‐like chain. These chains are decorated by PTCP ligands and form unique three zipper‐like structures, which are further assembled into three‐dimensional supramolecular nets by π···π stacking interactions. Additionally, hydrogen bonds are observed in the structures. Furthermore, compounds 1–3 were studied by IR spectrocopy and thermogravimetric analyses.

Url:

https://api.istex.fr/document/64F536190EE72E2B223AD8ED80B997757D7EE9BB/fulltext/pdf

DOI: 10.1002/zaac.201000386

Affiliations:

République populaire de Chine

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Le document en format XML

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<front><div type="abstract">Reaction of the ligands 2‐phenyl‐1H‐1,3,7,8‐tetraazacyclopenta[l]phenanthrene (PTCP) and benzene‐1,3‐dicarboxylic acid (m‐H2BDC) with Ln2O3 under hydrothermal conditions lead to three isomorphous coordination polymers [Ln2(PTCP)2(m‐BDC)3·H2O]n (Ln = Tm, 1; Nd, 2; Ce, 3). The coordination polymers crystallize in monoclinic, space group P21/m with a = 9.8340(2), b = 17.9140(4), c = 15.6050(3) Å, β = 100.51(3)° for 1, with a = 9.8423(3), b = 18.3562(4), c = 15.6209(3) Å, β = 102.138(3)° for 2, and with a = 9.8620(2), b = 18.4960(4), c = 15.6530(3) Å, β = 102.42(3)° for 3, respectively. The metal ions (Ln3+) are located in an octacoordinated environment and the dinuclear [Ln2O12N4] units act as octahedral secondary building units (SBU), which are bridged in two coordination modes by six m‐BDC ligands to form a three‐strand‐like chain. These chains are decorated by PTCP ligands and form unique three zipper‐like structures, which are further assembled into three‐dimensional supramolecular nets by π···π stacking interactions. Additionally, hydrogen bonds are observed in the structures. Furthermore, compounds 1–3 were studied by IR spectrocopy and thermogravimetric analyses.</div>
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Synthesis and Characterization of Three New Zipper‐like Lanthanide [Ln = TmIII, NdIII, CeIII] Coordination Polymers Containing 1,3‐Benzenedicarboxylate and 2‐Phenyl‐1H‐1,3,7,8‐tetraazacyclopenta[l]phenanthrene Ligands

Synthesis and Characterization of Three New Zipper‐like Lanthanide [Ln = TmIII, NdIII, CeIII] Coordination Polymers Containing 1,3‐Benzenedicarboxylate and 2‐Phenyl‐1H‐1,3,7,8‐tetraazacyclopenta[l]phenanthrene Ligands

Source :

Descripteurs français

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

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